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Hye Sung Kim 1 Article
Effect of Sintering Temperature on the Microstructure and Mechanical Properties of Solid Oxide Fuel Cell Anode Fabricated by Spark Plasma Sintering
Byung Ju Song, Ka Ram Kim, Hye Sung Kim
J Powder Mater. 2013;20(6):425-431.
DOI: https://doi.org/10.4150/KPMI.2013.20.6.425
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Microstructural and mechanical properties of Ni-YSZ fabricated using SPS processing have been investigated at various sintering temperatures. Our study shows samples to be applied as a SOFC anode have the proper porosity of 40% and high hardness when processed at 1100°C. These results are comparable to the values obtained at 100-200°C higher sintering temperature reported by others. This result is important because when the fabrication processes are performed above 1100°C, the mechanical property starts to decrease drastically. This is caused by the fast grain coarsening at the higher temperature, which initiates a mismatch between thermal expansion coefficients of Ni and YSZ and induces cracks as well.

Journal of Powder Materials : Journal of Powder Materials